National Pesticide Residue Control Plan (according to Art of Reg. (EC) No 396/2005)

Transcription

1 EESTI VABARIIK VETERINAAR- JA TOIDUAMET REPUBLIC OF ESTONIA VETERINARY AND FOOD BOARD National Pesticide Residue Control Plan (according to Art of Reg. (EC) No 396/2005) Country: Estonia Year: 2012 Part 1: Infrastructure of services involved in the implementation of the pesticide residue control plan Table 1. The list of organisations/agencies involved in the national pesticide residue control programme. Role Organisation name Organisation Address Official Reporting Organisation Veterinary and Food Board Väike-Paala street 3, Tallinn, Harjumaa, Estonia Residue programme design Sample Collection Laboratory services Veterinary and Food Board Agricultural Board Veterinary and Food Board Agricultural Board Agricultural Research Centre Laboratory for Residues and Contaminants Health Board Tartu Laboratory Väike-Paala street 3, Tallinn, Harjumaa, Estonia Teaduse street 2, Saku, Harjumaa, Estonia Väike-Paala street 3, Tallinn, Harjumaa, Estonia Teaduse street 2, Saku, Harjumaa, Estonia Teaduse street 4/6, Saku, Harjumaa, Estonia Põllu street 1a, Tartu, Tartumaa, Estonia All of plant origin Sample collection at production/processing, retail and storage level Sample collection at primary production level of plant origin All Veterinary and Food Board Väike-Paala street 3, Tallinn, Harjumaa, Estonia Enforcement agencies Agricultural Board Teaduse street 2, Saku, Harjumaa, Estonia ESTONIA Phone Fax Homepage vet@vet.agri.ee

2 Part 2: Design of monitoring plan Pesticide Residue Control Plan for the year 2012 is laid down in Commission Regulation No 915/2010, concerning the coordinated multiannual community control program of the Union for 2011, 2012 and 2013 to ensure compliance with maximum residue levels and to assess the consumer exposure to pesticide residues in and on food of plant and animal origin. Estonian national monitoring program contains a minimum number of samples to be taken and analyzed according to Commission Regulation No 915/2010 and it also includes risk based sampling plan provided by Agricultural Board (AB) and Veterinary and Food Board (VFB). In the year 2012 the VFB sampling plan contains the commodities laid down in the Regulation 915/2010 and vegetable based baby food samples (see Table 2. The national sampling plan for year 2012). Sampling is part of the routine surveillance activity. Inspectors of the VFB county centers carry out sampling for residues of foodstuffs in the context of food control activity according to the provisions of the law and by the monitoring plan and guide prepared by VFB central office. Samples are taken using the sampling method outlined in Commission Directive 2002/63/EC for the official control of pesticide residues. Samples (according to VFB plan) are planned to be taken from storage (S), retail (R), processing/production (P) level. Where possible the samples are taken randomly at storage level. The number of samples to be taken from domestic or imported foodstuff is depending on the availability of the foodstuffs on the market. While a relatively high percentage of fruits origin from Third countries (TC), it is not possible to predict the actual numbers of domestic or European Union (EU) or TC samples of certain foodstuffs. In 2012 there is an opportunity to analyze many samples of commodities which are originated from TC (e.g. table grapes, orange juice and bananas). But some of the commodities are suitable to take samples from domestic production (e.g. wheat, chicken eggs, cauliflower) and from EU production (e.g. peppers, olive oil, chicken eggs, broccoli). The number of organic products to be analyzed is depending from the actual market situation and from the crops harvested by farmers. Sampling plan of surveillance of use of plant protection products will be drawn up by AB at primary production (PP) level. AB s sampling plan is based on evaluated risks and results of previous year s sampling, attached in annual control plan. Crops cultivated each year and Estonians eating habits are also included. Sampling for residues of use of plant protection products of plant origin foodstuff is carried out by inspectors of AB county centers. Samples are taken using the sampling method outlined in Commission Directive 2002/63/EC for the official control of pesticide residues. The analytical results of surveillance of use of plant protection products will be included in the pesticide monitoring program at the end of the year The exact numbers of samples per commodity are not yet finite and will be corrected after finishing this years sampling and analyzing the results and risks. The commodities of organic products to be analyzed is depending from the crops harvested by farmers. See for details from Table 2. The national sampling plan for year

3 Table 2. The national sampling plan for year Class Commodity Sampling Point Number Samples Domestic Samples Veterinary and Food Board Plant products aubergines S, R 15 bananas S, R 15 0 broccoli S, R 7 cauliflower S, R 8 table grapes S, R 15 0 orange juice P, S, R peas without pod (fresh or S, R frozen) sweet peppers S, R 15 wheat P, S, R 15 olive oil P, S, R 15 Animal products butter P, S 15 chicken egg S, R 15 Infant and processed vegetable-based foods P, S, R 5 babyfood processed cereal-based foods P, S, R 10 Organic products plant products, infant and baby P, S, R food Total number of 180 VFB samples Class Commodity Sampling Number Domestic Point Samples Samples Agricultural Board Plant products potato PP vegetables PP berries PP oil seeds PP Organic products plant products PP Total number of AB samples Total number of samples 300 Imported Samples Imported Samples 3

4 Part 3: Analytical Methods and Quality Assurance Two laboratories analyze the samples: Health Board Tartu laboratory in Tartu (HB) and Agricultural Research Centre Laboratory for Residues and Contaminants in Saku (ARC). The laboratories are accredited by the Estonian Accreditation Centre (EAK) for all analytical methods used for official control of pesticide residues in food. All certificates of the accreditation can be found on the website of the EAK ( The EC guidelines SANCO/2007/3131 Method Validation and Quality Control procedures for Pesticide Residues have been implemented as far as practicable. The ARC laboratory uses multi-residue method for pesticide residue analysis in food of plant origin and a single residue method for determination of dithiocarbamates from food of plant origin; glyphosate, chlormequat and mepiquat residues in cereals. The list of residues which the laboratory analyzes is given in Table 3. The HB Tartu laboratory uses multi-residue method for pesticide residues analysis in food of plant and animal origin and in baby food. A single residue method is used for determination of dithiocarbamates in food. The list of residues which the laboratory analyzes is given in Table 4. During each year both laboratories plan to add analytes to their multi-residue methods and therefore the lists which are given in tables 3 and 4 are not complete for the year Unfortunay in many cases the residue definitions can not be achieved by laboratories because some metabolites are unstable and are difficult to detect and therefore difficult to add to the multi-residue methods. Table 3. List of residues and compounds analyzed by the Agricultural Research Centre Laboratory for Residues and Contaminants. Agricultural Research Centre Laboratory for Residues and Contaminants Plant Residue LOQ Abamectin (Avermectin B1a+Avermectin B1b) 0,005 Acephate 0,005 Acetamiprid 0,005 Aclonifen 0,01 Acrinathrin 0,01 Aldicarb (summa) 0,005 Aldicarb 0,005 Aldicarb sulfone 0,005 Aldicarb sulfoxide 0,005 Alphamethrin 0,01 Amidosulfuron 0,005 Amitraz, ka. metaboliidid DMF ja DMPF (2,4-dimethylformanilide ja N-2,4-dimethylphenyl-Nmethyl-formamidine) 0,005 Atrazine 0,01 Azinphos-ethyl 0,01 Azinphos-methyl 0,01 Azoxystrobin 0,01 Benalaxyl 0,005 Bentazone 0,01 Bifenox 0,01 Bifenthrin 0,01 Biphenyl* 0,01 4

5 Agricultural Research Centre Laboratory for Residues and Contaminants Residue Plant LOQ Bitertanol 0,01 Boscalid 0,01 Bromophos 0,005 Bromophos-ethyl 0,005 Bromopropylate 0,01 Bromuconazole 0,01 Bupirimate 0,01 Buprofezin 0,01 Cadusafos 0,01 Captan 0,01 Carbaryl 0,01 Carbendazim 0,005 Carbofuran (summa) 0,005 Carbofuran 0,005 Carbofuran, 3-hydroxy 0,005 Carboxin 0,01 Chlorfenapyr 0,01 Chlorfenvinphos 0,01 Chloridazone 0,005 Chlormephos 0,01 Chlorobenzilate 0,01 Chlorothalonil 0,01 Chlorpropham (summa) 0,01 Chlorpropham 0,01 3-chloroaniline 0,01 Chlorpyrifos 0,01 Chlorpyrifos-methyl 0,01 Chlorsulfuron 0,005 Clofentezine 0,005 Clomazone 0,005 Clopyralid 0,04 Clozolinate 0,01 Cyanazine 0,01 Cyazofamid 0,005 Cycloxydim 0,04 Cyfluthrin 0,01 λ-cyhalothrin 0,01 Cymoxanil 0,005 Cypermethrin (summa) 0,01 Cypermethrin 0,01 beta-cypermethrin 0,01 Cyproconazole 0,04 Cyprodinil 0,01 2,4-D (summa) 0,01 2,4-D 0,01 2,4-D 2-EHE 0,01 DDT (summa) 0,01 4,4-DDD 0,01 4,4-DDE 0,01 2,4-DDT 0,01 4,4-DDT 0,01 5

6 Agricultural Research Centre Laboratory for Residues and Contaminants Residue Plant LOQ Deltamethrin 0,01 Demeton-S-methyl 0,005 Oxydemeton-methyl 0,005 Demeton-S-methylsulfone 0,005 Demeton-S-methylsulfoxid 0,005 Desmedipham 0,005 Desmetryn 0,01 Diafenthiuron 0,01 Diazinon 0,01 Dicamba 0,04 Dichlofluanid 0,01 Dichlorvos 0,01 Dichlorprop 0,01 Diclofop-methyl 0,01 Dicloran 0,01 Dicofol 0,01 Dicrotophos 0,005 Dieldrin (summa) 0,01 Aldrin 0,005 Dieldrin 0,01 Diethofencarb 0,005 Difenoconazole 0,01 Diflubenzuron 0,04 Diflufenican 0,01 Dimethachlor 0,01 Dimethoate (summa) 0,01 Dimethoate 0,01 Omethoate 0,005 Dimethomorph 0,01 Dimoxystrobin 0,01 Dinocap 0,005 Diphenylamine 0,01 Disulfuton 0,01 Endosulfan (summa) 0,005 α-endosulfan 0,005 β-endosulfan 0,005 Endosulfan-sulfate 0,005 Endrin 0,005 EPN 0,01 Epoxiconazole 0,01 Ethiofencarb 0,005 Ethion 0,01 Ethofumesate 0,01 Ethoprophos 0,01 Etofenprox 0,005 Etrimfos 0,01 Famoxadone 0,01 Fenamidone 0,01 Fenamiphos (summa) 0,01 Fenamiphos 0,005 Fenamiphos-sulfone 0,005 6

7 Agricultural Research Centre Laboratory for Residues and Contaminants Residue Plant LOQ Fenamiphos-sulfoxide 0,01 Fenarimol 0,01 Fenazaquin 0,005 Fenbuconazole 0,005 Fenchlorphos 0,01 Fenhexamid 0,01 Fenitrothion 0,01 Fenoxaprop-P-ethyl 0,005 Fenoxycarb 0,01 Fenpropathrin 0,01 Fenpropidin 0,01 Fenpropimorph 0,01 Fenthion (summa) 0,01 Fenthion 0,01 Fenthion-sulfone 0,01 Fenthion-sulfoxide 0,005 Fenthion oxon 0,005 Fenthion oxon sulfone 0,005 Fenthion oxon sulfoxide 0,005 Fenvalerate/ Esfenvalerate summa 0,01 Fenvalerate 0,01 Esfenvalerate 0,01 Fipronil (summa)ü 0,01 Fipronil 0,005 Fipronil sulfone 0,01 Florasulam 0,005 Fluazifop 0,005 Fluazifop-P-buthyl 0,01 Fluazinam 0,005 Flucythrinate 0,01 Fludioxonil 0,01 Flufenoxuron 0,005 Fluopicolide 0,01 Fluoxastrobin 0,01 Fluroxypyr 0,01 Fluquinconazole 0,01 Flusilazole 0,01 Flutriafol 0,01 tau-fluvalinate 0,01 Folpet 0,01 Formothion 0,01 Fosthiazate 0,005 Fuberidazole 0,005 Furathiocarb 0,01 Haloxyfop (summa) 0,01 Haloxyfop 0,01 Haloxyfop-R-ME 0,01 Hexachlorobenzene (HCB) 0,005 HCH (summa) 0,005 α-hch 0,005 β-hch 0,005 7

8 Agricultural Research Centre Laboratory for Residues and Contaminants Residue Plant LOQ γ-hch (lindane) 0,005 Heptachlor (summa) 0,01 Heptachlor 0,01 cis-heptachlorepoxide 0,005 trans-heptachlorepoxide 0,005 Heptenophos 0,01 Hexaconazole 0,01 Hexaflumuron 0,01 Hexythiazox 0,005 Imazalil 0,01 Imazapyr 0,005 Imidacloprid 0,005 Indoxacarb 0,01 Iodosulfuron-methyl-sodium 0,005 Iprodione 0,01 Iprovalicarb 0,005 Isofenphos 0,01 Isofenphos-methyl 0,01 Isoprothiolane 0,01 Isoproturon 0,005 Krezoxim-methyl 0,01 Lenacil 0,005 Linuron 0,005 Lufenuron 0,005 Malathion (summa) 0,01 Malaoxon 0,01 Malathion 0,01 Mandipropamid 0,005 MCPA (summa) 0,01 MCPA 0,005 MCPB 0,01 Mecarbam 0,01 Mecoprop 0,01 Mepanipyrim 0,01 Mesosulfuron-methyl 0,005 Metaflumizone 0,01 Metalaxyli ja metalaxyl-m summa 0,01 Metalaxyl 0,01 Metalaxyl-M 0,005 Metamitron 0,01 Metazachlor 0,01 Metconazole 0,005 Methacrifos 0,01 Methamidophos 0,005 Methidathion 0,01 Methiocarb (summa) 0,005 Methiocarb 0,005 Methiocarb sulfone 0,005 Methiocarb sulfoxide 0,005 Methomyl (summa) 0,005 Methomyl 0,005 8

9 Agricultural Research Centre Laboratory for Residues and Contaminants Residue Plant LOQ Thiodicarb 0,005 Methoxyfenozide 0,005 Metobromuron 0,005 Metolachlor 0,005 Metrafenone 0,01 Metribuzin 0,01 Mevinphos 0,01 Monocrotophos 0,005 Monolinuron 0,005 Myclobutanil 0,01 Napropamide 0,01 Nicosulfuron 0,005 Nitenpyram 0,005 Oxadixyl 0,01 Oxamyl 0,005 Paclobutrazol 0,005 Parathion-methyl (summa) 0,01 Paraoxon-methyl 0,01 Parathion-methyl 0,01 Parathion-ethyl 0,01 Penconazole 0,01 Pencycuron 0,005 Pendimethalin 0,01 Permethrin 0,01 Phenmedipham 0,005 Phenthoate 0,01 2-phenylphenol* 0,01 Phorate 0,01 Phosalone 0,01 Phosmet 0,01 Phosmet 0,01 Phosmet oxon 0,01 Phosphamidone 0,01 Phoxim 0,005 Picolinafen 0,01 Picoxystrobin 0,01 Pinoxaden 0,005 Piperonyl-butoxide 0,005 Pirimicarb (summa) 0,01 Pirimicarb 0,01 Pirimicarb-desmethyl 0,01 Pirimiphos-methyl 0,01 Prochloraz (summa) 0,01 Prochloraz 0,01 2,4,6-trichlorophenol 0,01 Procymidone 0,01 Profenofos 0,01 Prometryn 0,01 Propachlor 0,01 Propamocarb 0,005 Propaquizafop 0,005 9

10 Agricultural Research Centre Laboratory for Residues and Contaminants Residue Plant LOQ Propargite* 0,01 Propazine 0,005 Propham 0,05 Propiconazole 0,01 Propoxur 0,005 Propoxycarbazone-Na 0,005 Propyzamide 0,01 Prosulfocarb 0,005 Prothioconazole (-desthio) 0,005 Prothiophos 0,01 Pyraclostrobin 0,01 Pyrazophos 0,01 Pyridaben 0,005 Pyridate 0,005 Pyrimethanil 0,01 Pyriproxyfen 0,005 Pyroxsulam 0,005 Quinalphos 0,01 Quinclorac 0,01 Quinmerac 0,005 Quinoxyfen 0,01 Quintozene 0,005 Quizalofop (summa) 0,01 Quizalofop-ethyl 0,005 Quizalofop-P-tefuryl 0,01 Rimsulfuron 0,005 Simazine 0,01 Spinosad (Spinosyn A ja Spinosyn D summa) 0,005 Spiroxamine 0,005 Sulfosulfuron 0,01 Zoxamide 0,01 Tebuconazole 0,01 Tebufenozide 0,005 Tebufenpyrad 0,005 Tecnazene 0,01 Teflubenzuron 0,005 Tefluthrin 0,01 Terbutryn 0,01 Terbuthylazine 0,005 Tetraconazole 0,01 Tetradifon 0,01 Thiabendazole 0,005 Thiacloprid 0,005 Thiamethoxam (summa) 0,01 Clothianidin 0,005 Thiamethoxam 0,01 Thifensulfuron-methyl 0,005 Thiophanate-methyl 0,01 Thiometon 0,01 Tolclofos-methyl 0,01 Tolylfluanid (summa) 0,04 10

11 Agricultural Research Centre Laboratory for Residues and Contaminants Residue Plant LOQ Tolylfluanid 0,01 DMST 0,04 Tralkoxydim 0,005 Triadimefon/Triadimenol summa 0,01 Triadimefon 0,01 Triadimenol 0,01 Triasulfuron 0,005 Triazamate 0,01 Triazophos 0,01 Trichlorphon 0,01 Tricyclazole 0,005 Trifloxystrobin 0,01 Triflumuron 0,04 Trifluralin 0,01 Trinexapac-ethyl 0,01 Triticonazole 0,01 Tritosulfuron 0,005 Vinclozolin 0,01 11

12 Tabel 4. List of residues and compounds analyzed by the Health Board Tartu Laboratory. Plant Animal Babyfood Health Board Tartu Laboratory Residue Incl LOQ Incl LOQ Incl LOQ 4,4 - Methoxychlor x 0,001 Acibenzolar-S-Methyl x 0,005 x 0,005 Aclonifen x 0,005 x 0,005 Acrinathrin x 0,005 x 0,005 Alachlor x 0,005 x 0,005 Aldrin x 0,005 x 0,001 x 0,005 Amitraz x 0,005 x 0,005 Aramite x 0,005 x 0,005 Azinphos-Ethyl x 0,005 x 0,001 x 0,005 Azinphos-Methyl x 0,005 x 0,005 Azoxystrobin x 0,005 x 0,005 Atrazine x 0,005 x 0,005 Benalaxyl x 0,005 x 0,005 Bendiocarb x 0,005 x 0,005 Bifenthrin x 0,005 x 0,001 x 0,005 Binapacryl x 0,005 x 0,005 Biphenyl x 0,005 x 0,005 Bitertanol x 0,005 x 0,005 Boscalid x 0,005 x 0,005 Bromophos-Ethyl x 0,005 x 0,005 Bromophos-Methyl x 0,005 x 0,005 Bromopropylate x 0,005 x 0,005 Bupirimat x 0,005 x 0,005 Buprofezin x 0,005 x 0,005 Cadusafos x 0,005 x 0,005 Captafol x 0,005 x 0,005 Captan x 0,005 x 0,005 Carbaryl x 0,005 x 0,005 Carbofuran x 0,005 x 0,005 Carbosulfan x 0,005 x 0,005 Chinometionat x 0,005 x 0,005 Chlorbenzide x 0,005 x 0,005 Chlorbufam x 0,005 x 0,005 Chlordane, trans- x 0,005 x 0,001 x 0,005 Chlorfenapyr x 0,005 x 0,005 Chlorfenzon x 0,005 x 0,005 Chlorfenvinphos x 0,005 x 0,005 Chlorobenzilate x 0,005 x 0,001 x 0,005 Chlorothalonil x 0,005 x 0,005 Chlorpropham x 0,005 x 0,005 Chlorpyrifos x 0,005 x 0,001 x 0,005 Chlorpyrifos-Methyl x 0,005 x 0,001 x 0,005 Chlorthal-Dimethyl x 0,005 x 0,005 Chlortiophos x 0,005 x 0,005 Chordane, cis- x 0,005 x 0,001 x 0,005 Cinidon-Ethyl x 0,005 x 0,005 Chlordane, oxy- x 0,005 x 0,001 x 0,005 Clozolinate x 0,005 x 0,005 Cyanazine x 0,005 x 0,005 Cyanofenphos x 0,005 x 0,005 12

13 Plant Animal Babyfood Health Board Tartu Laboratory Residue Incl LOQ Incl LOQ Incl LOQ Cyfluthrin x 0,005 x 0,001 x 0,005 Cyhalothrin, lambda- x 0,005 x 0,005 Cypermethrin x 0,005 x 0,001 x 0,005 Cyproconazole x 0,005 x 0,005 Cyprodinil x 0,005 x 0,005 Cyromazine x 0,005 x 0,005 DDD-o,p x 0,005 x 0,001 x 0,005 DDD-p,p x 0,005 x 0,001 x 0,005 DDE-o,p x 0,005 x 0,001 x 0,005 DDE-p,p x 0,005 x 0,001 x 0,005 DDT-o,p x 0,005 x 0,001 x 0,005 DDT-p,p x 0,005 x 0,001 x 0,005 Deltamethrin x 0,005 x 0,001 x 0,005 Desmethylpirimicarb x 0,005 x 0,005 Desmetryn x 0,005 x 0,005 Diallate x 0,005 x 0,005 Diazinon x 0,005 x 0,001 x 0,005 Dichlofluanid x 0,005 x 0,005 Diclobenil x 0,005 x 0,005 Diclofop-Methyl x 0,005 x 0,005 Dicloran x 0,005 x 0,005 Diclorvos x 0,005 x 0,005 Dicofol x 0,005 x 0,005 Dicrotophos x 0,005 x 0,005 Dieldrin x 0,005 x 0,001 x 0,005 Difenoconazole x 0,005 x 0,005 Dimetachlor x 0,005 x 0,005 Dimethoate x 0,005 x 0,005 Dimetomorph x 0,005 x 0,005 Dioxathion x 0,005 x 0,005 Diphenylamine x 0,005 x 0,005 Disulfoton x 0,005 x 0,005 Endosulfan, alpha x 0,005 x 0,001 x 0,005 Endosulfan, beta x 0,005 x 0,001 x 0,005 Endosulfansulfate x 0,005 x 0,001 x 0,005 Endrin x 0,005 x 0,001 x 0,005 EPN x 0,005 x 0,005 Epoxyconazole x 0,005 x 0,005 Ethion x 0,005 x 0,005 Etofenprox x 0,005 x 0,005 Etofumezate x 0,005 x 0,005 Etoprophos x 0,005 x 0,005 Etrimfos x 0,005 x 0,005 Fenamidon x 0,004 x 0,004 Fenamiphos x 0,005 x 0,005 Fenarimol x 0,005 x 0,005 Fenazaquin x 0,005 x 0,005 Fenchlorphos x 0,005 x 0,005 Fenhexamid x 0,005 x 0,005 Fenitrotion x 0,005 x 0,005 Fenobucarb x 0,005 x 0,005 13

14 Plant Animal Babyfood Health Board Tartu Laboratory Residue Incl LOQ Incl LOQ Incl LOQ Fenpropatrin x 0,005 x 0,005 Fenpropiomorph x 0,005 x 0,005 Fenthion x 0,005 x 0,001 x 0,005 Fenvalerate/Esfenvalerate1 (RR/SS) x 0,005 x 0,001 x 0,005 Fenvalerate/Esfenvalerate2 (RS/SR) x 0,005 x 0,001 x 0,005 Fipronil x 0,005 x 0,005 Flucythrinate x 0,005 x 0,005 Fludioxonil x 0,005 x 0,005 Flumioxazin x 0,005 x 0,005 Fluquinconazole x 0,005 x 0,005 Flusilazole x 0,005 x 0,005 Flutriafol x 0,005 x 0,005 Fluvalinate, tau- x 0,005 x 0,005 Folpet x 0,005 x 0,005 Formothion x 0,005 x 0,005 Fuberidazole x 0,005 x 0,005 Furathiocarb x 0,005 x 0,005 HCB x 0,005 x 0,001 x 0,005 HCH, alpha x 0,005 x 0,001 x 0,005 HCH, beta x 0,005 x 0,001 x 0,005 HCH, delta x 0,005 x 0,001 x 0,005 HCH, gamma x 0,005 x 0,001 x 0,005 Heptachlor x 0,005 x 0,001 x 0,005 Heptachlorepoxide, cis x 0,005 x 0,001 x 0,005 Heptachlorepoxide, trans x 0,005 x 0,001 x 0,005 Heptenophos x 0,005 x 0,005 Hexaconazole x 0,005 x 0,005 Hexythiazox x 0,005 x 0,005 Iprodione x 0,005 x 0,005 Iprovalicarb x 0,005 x 0,005 Isofenphos-Methyl x 0,005 x 0,005 Kresoxim-Methyl x 0,005 x 0,005 Lenacil x 0,005 x 0,005 Malaoxon x 0,005 x 0,005 Malathion x 0,005 x 0,005 Mecarbam x 0,005 x 0,005 Mepanipyrim x 0,005 x 0,005 Metacriphos x 0,005 x 0,005 Metalaxyl x 0,005 x 0,005 Metalaxyl-M x 0,005 x 0,005 Metazachlor x 0,005 x 0,005 Metidation x 0,005 x 0,001 x 0,005 Metoxychlor x 0,005 x 0,005 Metribuzin x 0,005 x 0,005 Mevinphos x 0,005 x 0,005 Monocrotophos x 0,005 x 0,005 Monolinuron x 0,005 x 0,005 Myclobutanil x 0,005 x 0,005 Nitrofen x 0,005 x 0,005 Nuarimol x 0,005 x 0,005 Omethoate x 0,005 x 0,005 14

15 Plant Animal Babyfood Health Board Tartu Laboratory Residue Incl LOQ Incl LOQ Incl LOQ Orthophenylphenol x 0,005 x 0,005 Paclobutrazole x 0,005 x 0,005 Paraoxon-methyl x 0,005 x 0,001 x 0,005 Parathion-Ethyl x 0,005 x 0,001 x 0,005 Parathion-Methyl x 0,005 x 0,001 x 0,005 Penconazole x 0,005 x 0,005 Pencycuron x 0,005 x 0,005 Pendimetalin x 0,005 x 0,005 Pentachloroaniline x 0,005 x 0,005 Pentachloroanizole x 0,005 x 0,005 Pentachlorobenzene x 0,005 x 0,005 Permethrin x 0,005 x 0,001 x 0,005 Phentoate x 0,005 x 0,005 Phorate x 0,005 x 0,005 Phosalone x 0,005 x 0,005 Phosmet x 0,005 x 0,005 Phosphamidon x 0,005 x 0,005 Picolinafen x 0,005 x 0,005 Pirimicarb x 0,005 x 0,005 Pirimiphos-Methyl x 0,005 x 0,001 x 0,005 Prochloraz x 0,005 x 0,005 Procymidon x 0,005 x 0,005 Profenofos x 0,005 x 0,001 x 0,005 Prometryn x 0,005 x 0,005 Propachlor x 0,005 x 0,005 Propargite x 0,005 x 0,005 Propiconazole x 0,005 x 0,005 Propoxur x 0,005 x 0,005 Propyzamide x 0,005 x 0,005 Prothiophos x 0,005 x 0,005 Pymetrozine x 0,005 x 0,005 Pyraclostrobin x 0,005 x 0,005 Pyraflufen-Ethyl x 0,005 x 0,005 Pyrazophos x 0,005 x 0,001 x 0,005 Pyridaben x 0,005 x 0,005 Pyrimethanil x 0,005 x 0,005 Pyriproxyfen x 0,005 x 0,005 Quinalphos x 0,005 x 0,005 Quinoxyfen x 0,005 x 0,005 Quintozene x 0,005 x 0,001 x 0,005 Resmethrin x 0,005 x 0,001 x 0,005 Simazine x 0,005 x 0,005 Spiroxamine x 0,005 x 0,005 Tebuconazole x 0,005 x 0,005 Tebufenpyrad x 0,005 x 0,005 Tecnazene x 0,005 x 0,001 x 0,005 Tefluthrin x 0,005 x 0,005 TEPP x 0,005 x 0,005 Terbutryn x 0,005 x 0,005 Tetraconazole x 0,005 x 0,005 Tetradifon x 0,005 x 0,005 15

16 Plant Animal Babyfood Health Board Tartu Laboratory Residue Incl LOQ Incl LOQ Incl LOQ Tolclofos-Methyl x 0,005 x 0,005 Tolylfluanid x 0,005 x 0,005 Triadimefon x 0,005 x 0,005 Triadimenol x 0,005 x 0,005 Triallate x 0,005 x 0,005 Triazophos x 0,005 x 0,001 x 0,005 Trifloxystrobin x 0,005 x 0,005 Trifluralin x 0,005 x 0,005 Vinclozolin x 0,005 x 0,005 Dithiocarbamates x 0,050 x 0,050 2,4,5-T x 0,010 x 0,010 2,4-D x 0,010 x 0,010 Acephate x 0,010 x 0,010 Acetamiprid x 0,010 x 0,010 Aldicarb x 0,020 x 0,020 Aldicarb-Sulfone x 0,010 x 0,010 Aldicarb-Sulfoxide x 0,010 x 0,010 Benomyl-group x 0,010 x 0,010 Bromuconazole x 0,010 x 0,010 Carbofuran-3-hydroxy x 0,010 x 0,010 Chloridazon x 0,010 x 0,010 Clofentezine x 0,010 x 0,010 Clopyralid x 0,010 x 0,010 Clothianidin x 0,010 x 0,010 Cymoxanil x 0,010 x 0,010 Demethon-S-methyl x 0,010 x 0,010 Demethon-S-methylsulfone x 0,010 x 0,010 Desmedipham x 0,010 x 0,010 Dinoseb x 0,010 x 0,010 Dinoterb x 0,010 x 0,010 Fenbuconazole x 0,010 x 0,010 Fenoxycarb x 0,010 x 0,010 Fluazifop x 0,010 x 0,010 Flufenoxyron x 0,010 x 0,010 Fluoroxypyr x 0,010 x 0,010 Formetanate x 0,010 x 0,010 Fosthiazate x 0,010 x 0,010 Haloxyfop x 0,010 x 0,010 Imazalil x 0,010 x 0,010 Imidacloprid x 0,010 x 0,010 Indoxacarb x 0,010 x 0,010 Ioxynil x 0,010 x 0,010 Isoproturon x 0,010 x 0,010 Linuron x 0,010 x 0,010 Lufenuron x 0,010 x 0,010 MCPA x 0,010 x 0,010 MCPB x 0,010 x 0,010 MCPP-P x 0,010 x 0,010 Metamitron x 0,010 x 0,010 Metconazole x 0,010 x 0,010 Methamidophos x 0,010 x 0,010 16

17 Plant Animal Babyfood Health Board Tartu Laboratory Residue Incl LOQ Incl LOQ Incl LOQ Methiocarb x 0,010 x 0,010 Methiocarb-Sulfone x 0,010 x 0,010 Methiocarb-Sulfoxide x 0,010 x 0,010 Methomyl x 0,010 x 0,010 Methoxyfenozide x 0,010 x 0,010 Metsulfuroonmetüül x 0,010 x 0,010 Oxadixyl x 0,010 x 0,010 Oxamyl x 0,010 x 0,010 Oxydemtehon-methyl x 0,010 x 0,010 Phenmedipham x 0,010 x 0,010 Phorate-Sulphone x 0,010 x 0,010 Propham x 0,010 x 0,010 Phoxim x 0,010 x 0,010 Pyridate x 0,010 x 0,010 Spinosad x 0,010 x 0,010 Zoxamide x 0,010 x 0,010 Tebufenozide x 0,010 x 0,010 Teflubenzuron x 0,010 x 0,010 Thiabendazole x 0,010 x 0,010 Thiacloprid x 0,010 x 0,010 Thiametoxam x 0,010 x 0,010 Thifensulfuron-methyl x 0,010 x 0,010 Thiodicarb x 0,010 x 0,010 Thiophanat-methyl x 0,010 x 0,010 Triasulfuron x 0,010 x 0,010 Triclorofon x 0,010 x 0,010 Triflumuron x 0,010 x 0,010 Triforin x 0,010 x 0,010 Triticonazole x 0,010 x 0,010 Vamidothion x 0,010 x 0,010 Part 4: Actions in response to non-complaint results In case of numerical exceedance no enforcement actions will be taken (if the result is below MRL after taking into account the analytical uncertainty and 50% of the result). In case of exceeding the MRL (as defined in the Regulation (EC) No 396/2005) enforcement actions will be taken. Competent authority VFB gives a precept (injunction) according to national Food Act and Regulation No 178/2002 and prohibits the handling or delivery to the final consumer of this particular unsafe food. The product will be withdrawn from the market, it is organized by that food business operator (for example food processor, wholesaler, importer) who s product was analyzed and the result was non-complaint. Whenever possible follow-up samples from the same food business operator s food are taken next year. When a result is numerically close to MRL or is numerically exceeding the MRL or is actually exceeding the MRL then a risk assessment is conducted and when appropriate a RASFF notification is issued. EFSA acute chronic model and Guidance Document on Notification criteria for pesticide residue findings to the Rapid Alert System for Food and Feed (RASFF) is used for the risk assessment. 17