Quality Services International GmbH. Testreport. Czech Honey Prokes Blanka M. Lukes Hajni 1363 CZ Prague Czech Republic
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1 QSI GmbH - D- Czech Honey Prokes Blanka M. Lukes Hajni 1363 CZ Prague Czech Republic Order No.: /12679 Date: 20-Dec-2016 Product: Honig/Honey Kind: Label: ohne/without Testreport Sample No: Sample Date: 20-Dec-2016 Packaging: Glas 500 ml Seal: ohne/without Printed: 21-Dec /1 Date: 21-Dec-2016 Temp.: RT The test results are exclusively related to the items tested for this sample. Method and measurement uncertainty details are available upon request. This report is allowed to be copied completely and unchanged but not in extracts. Test period: order date till date of this report Chemical-physical analysis (45153) Pyrrolizidine alkaloids (PA), BfR-PA-Honey-1.0/2013 with scope BfR-PA-Tea-2.0/2014, LC-MS/MS, honey Parameter in µg/kg LOQ* Result Sum of BfR-28 Pyrrolizidine Alkaloids* Sum of total Pyrrolizidine Alkaloids Echimidine* 1 Echimidine-N-Oxide* 1 Erucifoline* 5 Erucifoline-N-Oxide* 2 Heliotrine* 1 Heliotrine-N-Oxide* 1 Lycopsamine* 1 Lycopsamine-N-Oxide* 1 Europine* 1 Europine-N-Oxide* 1 Intermedine+further tert. Lycopsamine-Type PA* 1 Intermedin-N-Oxid* (+Indicin-N-Oxid and further LycTyp-PA-NOx) 1 Jacobine* 1 Jacobine-N-Oxide* 2 Senecionine* 1 Senecionine-N-Oxide* 1 Seneciphylline* 1 Seneciphylline-N-Oxide* 3 Senecivernine* 1 Senecivernine-N-Oxide* 1 Senkirkine* 1 Monocrotaline* 5 Monocrotaline-N-Oxide* 2 Lasiocarpine* 1 Lasiocarpine-N-Oxide* 1 Retrorsine* 1 Retrorsine-N-Oxide* 2 Riddelliine** 3 Riddelliine-N-Oxide** 5 Page: 1 of 4
2 Trichodesmine* 1 ** = no certified reference standard µg PA per 20 g Honey (one portion) µg BfR-PA* per 20 g Honey (one portion) * loq = limit of quantitation, = not detectable (below loq) Scope of PA according to BfR method 2.0/2014 for plant material. Chemical-physical analysis (45201) Antibiotics, Tetracyclines, LC-MS/MS, Honey Substance in [µg/kg] loq permitted level** Result Oxytetracycline (Terramycine R) 10 Tetracycline 10 Chlorotetracycline 10 Doxycycline 10 Methacycline 10 Minocycline 10 * loq = limit of quantitation; = below loq **no legal limit (MRL) acc. EU-Reg. 470/ /2010 means: no permit for use of antibiotics in beekeeping Chemical-physical analysis (45226) Antibiotic, Streptomycins, LC-MS/MS, Honey (loq 10 ppb) Parameter in [µg/kg] permitted level loq* result Streptomycine ** 10 Dihydrostreptomycine ** 10 * loq = limit of quantitation, = below loq ** not allowed as no MRL acc. EU-Regulation 470/ /2010 Under consideration of above indicated limit of quantitation the result of this sample complies with current EU-Regulation for veterinary medicinal products in foodstuff of animal origin. Page: 2 of 4
3 Chemical-physical analysis (45237) Antibiotics, Sulfonamides, Trimethoprim, LC-MS/MS, honey Substance in [µg/kg] permitted level** loq* result Sulfadimethoxin ** 5 Sulfaquinoxalin ** 5 Sulfachlorpyridazin ** 5 Sulfamoxol ** 5 Sulfadoxin ** 5 Sulfasalazin ** 5 Sulfabenzamid ** 5 Sulfaguanidin ** 5 Sulfanilamid ** 10 Sulfacetamid ** 5 Sulfadiazin ** 5 Sulfathiazol ** 5 Sulfapyridin ** 5 Sulfamerazin ** 5 Sulfamether ** 5 Sulfadimidin (= Sulfamethazin) ** 5 Sulfamethoxypyridazin ** 5 Sulfamethoxazol ** 5 Trimethoprim ** 5 Sulfamonomethoxin ** 5 Sulfaclozine ** 5 Sulfisoxazole ** 5 Succinylsulfatiazole ** 10 Sulfaphenazole ** 5 Sulfisozole ** 5 Sulfisomidine ** 5 * loq = limit of quantitation, = below loq **no legal limit (MRL) acc. EU-Reg. 470/ /2010 means: no permit for using antibiotics in beekeeping Chemical-physical analysis (45241) Antibiotic, Tylosine, LC-MS/MS (loq 2 ppb), honey Substance in [µg/kg] permitted level** loq* result Tylosine A 2 Tylosine B 2 * loq = limit of quantitation, = below loq **no legal limit (MRL) acc. EU-Regulation 37/2010 Annex Table 1: no permit of using Antibiotics in beekeeping Page: 3 of 4
4 Chemical-physical analysis (45305) Antibiotics, Nitrofuran Metabolites, LC-MS/MS (loq 1 ppb), Honey Substance in [µg/kg] perm. level (MRL)** loq* Result Semicarbazid (from Nitrofurazon) ** 1,0 AOZ (from Furazolidon) ** 1,0 AH (from Nitrofurantoin) ** 1,0 AMOZ (from Furaltadon) ** 1,0 * loq = limit of quantitation; = below loq MRPL (2003/181/EG) 1 µg/kg **Prohibited substance acc. EU-Regulation 37/2010 Annex Table 2 Chemical-physical analysis (86211) Chloramphenicol (CAP), LC-MS/MS, Honey (loq 0,3 ppb) Substance in [µg/kg=ppb] permitted level** loq* Result Chloramphenicol ** 0,3 * loq = limit of quantitation, / = below loq MRPL (2003/181/EC) = 0,3 µg/kg ** Prohibited substance acc. to EU Regulation 37/2010 Annex Table 2 This examination is the basis for special decision guidance. Authorized by: Annika Hoffmann Version 0 Page: 4 of 4
5 QSI GmbH - D- Czech Honey Prokes Blanka M. Lukes Hajni 1363 CZ Prague Czech Republic Order No.: /12679 Date: 20-Dec-2016 Product: Honig/Honey Kind: Label: ohne/without Testreport Sample No: Sample Date: 20-Dec-2016 Packaging: Glas 500 ml Seal: ohne/without Printed: 21-Dec /1 Date: 21-Dec-2016 Temp.: RT The test results are exclusively related to the items tested for this sample. Method and measurement uncertainty details are available upon request. This report is allowed to be copied completely and unchanged but not in extracts. Test period: order date till date of this report Chemical-physical analysis (88510) Pesticide-Residues, Glyphosate, LC/MS/MS, honey Parameter in mg/kg loq maximum residue level* Result Glyphosate 0,010 0,050 = below loq (limit of quantification) * according to Regulation (EC) No. 396/2005 With respect to our examination program the sample complies with current Regulation (EC) No. 396/2005. This examination is the basis for special decision guidance. Authorized by: Annika Hoffmann Version 0 Order No.: Customer No.: SN: Page: 1 of 1
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