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..8.897.8 9. 9.8 8.976 8.96 8.697 8.6 8. 8. 8. 7.8 7.8 7.8 7.78 7.76 7.67 7.68 7.69 7.9 7.7 LDN-989 NMR Analysis, Solvent= DMSO 68 MedKoo Cat Name LDN-989 CAS 668-- Lot CRB6 Exact Mass 6.99 Molecular Weight 6.8 LDN 989 6.9 spect mm PABBO BB zg 66 DMSO 6 8.68.8.98687 6 6.8 6. 98.. Hz Hz sec usec usec K sec ======== CHANNEL f ======== NUC H P.8 usec PL. db PLW.9668 W SFO.7 MHz SI 768 SF. MHz WDW EM SSB LB. Hz GB PC..8.6 8. 9..97.9.97..68.7. 7 6 ppm NAME EXPNO PROCNO Date_ Time INSTRUM PROBHD PULPROG TD SOLVENT NS DS SWH FIDRES AQ RG DW DE TE D TD

Data File F\LDN-989.D Sample Name LDN-989 LDN-989 HPLC Analysis Acq. Operator 系统 Seq. Line Acq. Instrument LC6 Location Vial 8 Injection Date //6 8 PM Inj Inj Volume µl Different Inj Volume from Sequence! Actual Inj Volume µl Acq. Method E\DATA\Yi zhijun\data\6\9-6-- --6\-9 AD MIN.M //6 6 PM by 系统 Analysis Method D\PUBLIC\6\DEF_LC 6-- -9-8\LXF-6-.D\DA.M (-9 6MIN.M) //6 8 PM by LXF-6- A.87 re a 7. 6 7 A6.77 re a. 6 9 7 A.6 re a 8. 97 7 8 Percent Report Sorted By Signal Multiplier. Dilution. Use Multiplier & Dilution Factor with ISTDs Signal VWD A, Wavelength= nm MedKoo Cat Name LDN-989 CAS 668-- Lot CRB6 Exact Mass 6.99 Molecular Weight 6.8.6 MM.76 8.9777.988.7.87 MM.676 7. 6.9 99.77 6.77 MM.8.697 6.99e-.79 Instrument //6 PM LXF-6- VWD A, Wavelength= nm (F\LDN-989.D) mau of

Data File F\LDN-989.D Sample Name LDN-989 LDN-989 HPLC Analysis Totals 8.8 67.8 *** End of Report *** MedKoo Cat Name CAS LDN-989 668-- Lot CRB6 Exact Mass 6.99 Molecular Weight 6.8 Instrument //6 PM LXF-6- of

Data File D\PUBLIC\6\DEF_LC 6-- 6--6\LDN-989.D Sample Name LDN-989 DAD A, Sig=, Ref=off (D\PUBLIC\6\DEF_LC 6-- 6--6\LDN-989.D) 8 6.68 mau LDN-989 MS Analysis Acq. Operator LXF-6- Seq. Line Acq. Instrument Instrument Location Vial Injection Date //6 9 PM Inj Inj Volume µl Different Inj Volume from Sequence! Actual Inj Volume µl Acq. Method D\Public\6\DEF_LC 6-- 6--6\-9 6MIN.M //6 8 AM by LXF-6- Analysis Method D\PUBLIC\6\DEF_LC 6-- -9-8\LXF-6-.D\DA.M (-9 6MIN.M) //6 8 PM by LXF-6- DAD B, Sig=,6 Ref=off (D\PUBLIC\6\DEF_LC 6-- 6--6\LDN-989.D) mau.68 MSD TIC, MS File (D\PUBLIC\6\DEF_LC 6-- 6--6\LDN-989.D) ES-API, Pos, Scan, Frag 7, "scan" 6 8 6 Instrument //6 PM LXF-6- MedKoo Cat Name LDN-989 CAS 668-- Lot CRB6 Exact Mass 6.99 Molecular Weight 6.8 of

Data File D\PUBLIC\6\DEF_LC 6-- 6--6\LDN-989.D Sample Name LDN-989 LDN-989 MS Analysis MSD TIC, MS File (D\PUBLIC\6\DEF_LC 6-- 6--6\LDN-989.D) ES-API, Neg, Scan, Frag 7, "scan" 9 8 7 6 Percent Report Sorted By Signal Multiplier. Dilution. Use Multiplier & Dilution Factor with ISTDs Signal DAD A, Sig=, Ref=off.68 VV.79 68.96 978.98. Totals 68.96 978.98.68 VV.7 67.98 9.99. Totals MedKoo Cat Name LDN-989 CAS 668-- Lot CRB6 Exact Mass 6.99 Molecular Weight 6.8 67.98 9.99 Signal MSD TIC, MS File Instrument //6 PM LXF-6- Signal DAD B, Sig=,6 Ref=off of

Data File D\PUBLIC\6\DEF_LC 6-- 6--6\LDN-989.D Sample Name LDN-989 LDN-989 MS Analysis *** End of Report *** MedKoo Cat Name LDN-989 CAS 668-- Lot CRB6 Exact Mass 6.99 Molecular Weight 6.8 Instrument //6 PM LXF-6- Signal MSD TIC, MS File of

Print of window 8 MS Spectrum LDN-989 HPLC Analysis MS Spectrum ES-API, Pos, Scan, Frag 7, "sc 7. *MSD SPC, time=.7 of D\PUBLIC\6\DEF_LC 6-- 6--6\LDN-989.D Max 67 7. 8. 79. 6 8. 8.. MedKoo Cat Name LDN-989 CAS 668-- Lot CRB6 Exact Mass 6.99 Molecular Weight 6.8 Instrument //6 9 PM LXF-6-6 7 m/z 8 of